I. |
Introduction |
I-1 |
I. |
(1) |
Definition of Macroanalytical Methods |
I-1 |
I. |
(2) |
Advantages and Limitations of Macroanalytical Methods |
I-1 |
I. |
(3) |
Scope of the Macroanalytical Procedures Manual |
I-2 |
I. |
(4) |
Legal Aspects |
I-2 |
I. |
(5) |
Determination of Defects |
I-1 |
I. |
(6) |
Sampling Methods |
I-1 |
II. |
Apparatus for Macroanalytical Methods |
II-1 |
III. |
Reagents for Macroanalytical Methods (PDF) |
III-1 |
IV. |
Special Techniques |
IV-1 |
IV. |
(1) |
X-Ray Radiography |
IV-1 |
IV. |
(2) |
Determination of the Direction of Insect Penetration of Food Packaging |
IV-2 |
IV. |
(3) |
Microscopic Confirmation of Decomposition and Rot |
IV-4 |
IV. |
(4) |
Detection and Recovery of Live Insects |
IV-4 |
V. |
Macroanalytical Methods |
V-1 |
V. |
1. |
Beverage and Beverage Materials |
V-1 |
V. |
|
A. |
Method for Coffee Beans |
V-1 |
V. |
2. |
Bakery Products, Cereals, and Alimentary Pastes |
V-12 |
V. |
|
A. |
Method for Bakery Products, Cooked Cereals, and Alimentary Pastes |
V-12 |
V. |
|
B. |
Method for Modified Whole Grains |
V-13 |
V. |
3. |
Whole Grains and Pseudo-Grains Updated May 2021 |
V-15 |
V. |
|
A. |
Method for Wheat, Corn, Popcorn Kernels, and Rice |
|
V. |
|
B. |
Method for Other Grains |
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V. |
|
C. |
Method for Pseudo-Grains |
|
V. |
4. |
Chocolate, Sugars, and Related Products |
V-18 |
V. |
|
A. |
Method for Cocoa Beans |
V-18 |
V. |
|
B. |
Method for Candy |
V-22 |
V. |
5. |
Miscellaneous and Multiple Food Products |
V-24 |
V. |
|
A. |
Method for Plant Gums |
V-24 |
V. |
6. |
Dairy, Cheese, and Related Products |
V-26 |
V. |
|
A. |
Method for Casein and Sodium Caseinate |
V-26 |
V. |
7. |
Seafood |
V-27 |
V. |
|
A. |
Method for Microscopic Detection of Fish Tissue in Crab Meat or Crab Cakes |
V-27 |
V. |
|
B. |
Method for Determination of Parasites in Fin Fish |
V-28 |
V. |
8. |
Spices, Condiments, Flavors, and Crude Drugs |
V-32 |
V. |
|
A. |
General Method for Spices, Herbs, and Botanicals |
V-32 |
V. |
|
B. |
Supplemental Method for Black and White Pepper |
V-39 |
V. |
|
C. |
SUPPLEMENTAL Method for Nutmegs |
V-41 |
V. |
9. |
Fruits and Fruit Products |
V-42 |
V. |
|
A. |
Method for Apple Products |
V-42 |
V. |
|
B. |
Method for Decomposition in Blackberries, Raspberries and Other Drupelet Berries |
V-44 |
V. |
|
C. |
Method for Decomposition in Blueberries |
V-46 |
V. |
|
D. |
Method for Cherries |
V-48 |
V. |
|
E. |
Method for Canned and Frozen Fruits |
V-51 |
V. |
|
F. |
Method for Dried Fruits |
V-53 |
V. |
|
G. |
Method for Grape Products |
V-59 |
V. |
|
H. |
Method for Jams, Preserves, and Jellies |
V-61 |
V. |
|
I. |
Method for Lingonberries |
V-64 |
V. |
|
J. |
Method for Mincemeat |
V-66 |
V. |
|
K. |
Method for Olives |
V-67 |
V. |
|
L. |
Method for Pineapple Products |
V-73 |
V. |
|
M. |
Method for Raisins |
V-76 |
V. |
|
N. |
Method for Processed Strawberries |
V-78 |
V. |
10. |
Nuts and Nut Products |
V-81 |
V. |
|
A. |
Method for In-shell and Shelled Tree Nuts |
V-81 |
V. |
|
B. |
Method for Peanuts and Peanut Siftings |
V-89 |
V. |
|
C. |
Method for Microscopic Detection of Foreign Plant Tissues in Peanut Butter |
V-92 |
V. |
11. |
Vegetables and Vegetable Products |
V-93 |
V. |
|
A. |
Method for Asparagus |
V-93 |
V. |
|
B. |
Method for Brussels Sprouts |
V-95 |
V. |
|
C. |
Method for Microscopic Detection of Substitute Vegetable Tissues in Ground Horseradish |
V-96 |
V. |
|
D. |
Method for Lettuce |
V-98 |
V. |
|
E. |
Method for Mushroom Products |
V-100 |
V. |
|
F. |
Method for the Reservation and Identification of Mushrooms |
V-102 |
V. |
|
G. |
Method for Peas and Beans (Canned, Frozen, and Dried) |
V-104 |
V. |
|
H. |
Method for Pickled Vegetables and Relish |
V-108 |
V. |
|
I. |
Method for Pimientos |
V-111 |
V. |
|
J. |
Method for Potato Chips |
V-113 |
V. |
|
K. |
Method for Corn Husks |
V-115 |
V. |
|
L. |
Method for Garlic Bulbs |
V-117 |
V. |
12. |
Cosmetic Products Updated March 2023 |
V-119 |
V. |
|
A. |
Method for Cosmetic Brushes |
V-119 |
VI. |
Applications of Macroanalytical Methods to Field Testing and Factory Samples |
VI-1 |
VI. |
(1) |
Introduction |
VI-1 |
VI. |
(2) |
Wharf Examination |
VI-1 |
VI. |
(3) |
Field applications of Macroanalytical Methods |
VI-2 |
VI. |
(4) |
Application of Macroanalytical Methods of Factory Samples |
VI-7 |
Glossary |
G-1 |
Index of Tables and Figures |
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